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Volatile Organic Compounds (VOCs) were extracted from fresh leaf tissue using headspace solid-phase microextraction (HS-SPME). Samples (5g) were homogenized with distilled water and calcium chloride to inhibit enzymatic activity. The extraction fiber (DVB/CAR/PDMS) was exposed to the headspace for 30 min at 40°C. Analysis was performed using an Agilent 7890B GC system coupled with a 5977B MSD. Identification of compounds was achieved by comparing mass spectra with the NIST library and authentic standards. ciboulette littlecib hot
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